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Crystal Optics - Polished Windows & Blanks
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Polished Crystal Optics - Disc
At ICL, we have been producing high quality crystal optics for use in infrared spectrometers, accessories, and other analytical devices since 1962. We are the only U.S. company that produces KBr crystal, a standard component of infrared spectrometers. In house, we also produce the materials for other vital crystal optics such as KCl, NaCl, AgCl, CdMnTe, and more. We also stock a large variety of spectroscopy optics made from other essentials like CaF2, BaF2, ZnS, ZnSe, Si, BK-7, etc. Circular Discs are available in all of the common sizes, typically in the range of 20mm-50mm (for use as windows common to infrared sample cells and accessories). However, we offer a large range of sizes for various applications, from tiny plugs for microscope slides to large aperture optical viewports (100mm in diameter or more).
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Polished Crystal Optics - Rectangle
At ICL, we have been producing high quality crystal optics for use in infrared spectrometers, accessories, and other analytical devices since 1962. We are the only U.S. company that produces KBr crystal, a standard component of infrared spectrometers. In house, we also produce the materials for other vital crystal optics such as KCl, NaCl, AgCl, CdMnTe, and more. We also stock a large variety of spectroscopy optics made from other essentials like CaF2, BaF2, ZnSe, ZnS, Si, BK-7, etc. Rectangular-shaped crystals are available in all of the common sizes frequently used in sealed liquid cells along with many other infrared sampling accessories.
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Unpolished Crystal Optics
Unpolished crystal optics are also known as blanks. These windows are finely ground with flat parallel surfaces. As sold they are opaque. They can be water polished quickly to achieve 90% transmission. The transmission of water polished KBr, KCI and NaCl will be the same as Real Crystal® IR Cards.These blanks can also be polished to precision optics. Blanks are ideal for mulls, smears and qualitative testing.
Quantity discounts and custom sizes are available. Ask for a quotation. -
Polyethylene Sheets
Polyethylene is a useful transmission material for far infrared sampling. Polyethylene is non-absorbing beyond 14 microns. Transmission is about 80%.
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Coated and Wedged Windows
High refractive index material such as ZnSe creates fringing, which is also known as channeling. Fringes are useful for path length calibration, but fringes can also interfere with spectral analysis, particularly when the refractive index of the sample is not well matched to the refractive index of the sample. Fringing can occur in a single window where the light is reflected between parallel surfaces of window and in a cell containing a pair of windows where the light is reflected off of both windows. The smaller the path length, the more dramatic the fringing effect is. Accordingly, thinner windows will have more dramatic fringes than thicker windows. Fig. 1 shows the fringe pattern of a properly assembled ZnSe 0.1mm path length liquid cell. This cell can be calibrated to a high degree of accuracy and has utility for well matched samples. But, if the sample is not well matched and ZnSe or some other high index material is chosen for reasons such as spectral range or material compatibility, then the spectroscopist may be well advised to consider means useful to limit fringing.
A simple way to limit fringing is to wedge the spacers in liquid cells. The downside is that the path length cannot be calibrated with the same high degree of accuracy that would otherwise be possible. This method works because the wedged spacer insures the windows are not parallel. There is an additional charge for the wedged spacer and the part number is 0001-9228.
Another simple way to limit fringes is to fog the windows. This of course only works with deliquescent windows which typically have a low refractive index anyway. Most windows that comprise the sample compartment seal in FTIR spectrophotometers are wedged KBr with a moisture barrier coating.
In gas cells, we provide windows that are both wedged and anti-reflective (AR) coated on one side. Prices for stock AR/wedged windows are shown below.
Broadband AR coatings also can be applied on both sides of a window, and are typically designated as AR/AR. Although AR coatings do have some spurious bands, they can generally be tolerated and can be compensated by means of a background scan of the sampling accessory containing the AR coated windows.
We routinely provide wedged windows in many materials. Wedged windows are the traditional and most inexpensive means of limiting fringing.